Synthesis of Magnesium- and Aluminum-Based Mixed Oxide Systems by Low and High Supersaturation Methods

V. V. Fadeev; Фадеев В. В.; A. P. Tronov; Тронов А. П.; A. V. Tolchev; Толчев А. В.; D. M. Galimov; Галимов Д. М.; V. E. Zhivulin; Живулин В. Е.; R. S. Morozov; Морозов Р. С.; V. V. Avdin; Авдин В. В.

doi:10.31857/S0044457X22602036

Synthesis of Magnesium- and Aluminum-Based Mixed Oxide Systems by Low and High Supersaturation Methods

Autores: Fadeev V.V.¹, Tronov A.P.¹, Tolchev A.V.¹, Galimov D.M.², Zhivulin V.E.², Morozov R.S.², Avdin V.V.²
Afiliações:
1. Chelyabinsk State University
2. South Ural State University
Edição: Volume 68, Nº 5 (2023)
Páginas: 613-622
Seção: СИНТЕЗ И СВОЙСТВА НЕОРГАНИЧЕСКИХ СОЕДИНЕНИЙ
URL: https://rjpbr.com/0044-457X/article/view/665255
DOI: https://doi.org/10.31857/S0044457X22602036
EDN: https://elibrary.ru/SNEVVM
ID: 665255

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Resumo

Magnesium–aluminum layered double hydroxides and mixed oxides based on them were obtained by high and low supersaturation methods and analyzed. It was shown that the phase composition and formation of nano-sized particles with a large surface area is significantly affected by the rate of introduction of magnesium–aluminum systems into the medium of the precipitated material. All of the obtained samples were studied by thermogravimetric analysis with mass-spectrometric detection, X-ray diffractometry, scanning electron microscopy, energy dispersive X-ray spectroscopy, and infrared spectroscopy.

Palavras-chave

layered double hydroxide, mixed oxide, magnesium, aluminum, nanoparticles, active surface area

Bibliografia

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