Synthesis of Boron Nitride by Reduction of Boron Oxide with Aluminum in Nitrogen

D. A. Tkachev; Ткачев Д. А.; M. Kh. Ziatdinov; Зиатдинов М. Х.; I. A. Zhukov; Жуков И. А.; V. A. Litvinova; Литвинова В. А.; I. A. Belchikov; Бельчиков И. А.; N. G. Kravtsov; Кравцов Н. Г.

doi:10.31857/S0044457X23600354

Synthesis of Boron Nitride by Reduction of Boron Oxide with Aluminum in Nitrogen

Авторлар: Tkachev D.A.¹, Ziatdinov M.K.¹, Zhukov I.A.¹, Litvinova V.A.², Belchikov I.A.¹, Kravtsov N.G.¹
Мекемелер:
1. Tomsk State University
2. Tomsk State University of Architecture and Building
Шығарылым: Том 68, № 10 (2023)
Беттер: 1405-1412
Бөлім: СИНТЕЗ И СВОЙСТВА НЕОРГАНИЧЕСКИХ СОЕДИНЕНИЙ
URL: https://rjpbr.com/0044-457X/article/view/666176
DOI: https://doi.org/10.31857/S0044457X23600354
EDN: https://elibrary.ru/AJOUQB
ID: 666176

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Аннотация
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Әдебиет тізімі
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Статистика

Аннотация

The paper presents the results of studies of the self-propagating high temperature synthesis (SHS) of boron nitride via chemical reduction of boron oxide with aluminum in a nitrogen medium. The phase composition of the powder reaction products depending on the nitrogen pressure during the synthesis was studied by X-ray diffraction. It was found that SHS in the B2O3–Al system gives the BN–Al2O3 powder material containing 20–28 wt % hexagonal boron nitride depending on the nitrogen pressure. Microstructure examination showed that the obtained powder materials contains separate hexagonal BN particles with <3 μm size. The differences in the density and morphology of BN and Al2O3 determine the possibility of BN isolation from the obtained powder mixture by the pneumatic powder separation methods.

Негізгі сөздер

self-propagating high-temperature synthesis, powder materials, hexagonal boron nitride, phase composition

Әдебиет тізімі

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