A New Method for the Synthesis of Layered Europium Hydroxide Using Propylene Oxide as the Precipitating Agent

Мұқаба

Дәйексөз келтіру

Толық мәтін

Ашық рұқсат Ашық рұқсат
Рұқсат жабық Рұқсат берілді
Рұқсат жабық Рұқсат ақылы немесе тек жазылушылар үшін

Аннотация

A new method for the synthesis of layered europium basic chloride in up to 90% yield was developed. The method is based on hydrolysis of europium chloride in the presence of propylene oxide. The effect of reaction temperature on the yield and composition of the products of europium chloride hydrolysis in the presence of propylene oxide was analyzed. The obtained layered europium basic chloride had pronounced anion exchange properties. The possibility of intercalation of the isonicotinate anion into a layered rare earth hydroxide was demonstrated for the first time. The intercalation of the benzoate or isonicotinate anions into layered europium hydroxide led to luminescence sensitization and decrease in the Eu3+ local symmetry.

Авторлар туралы

E. Sheichenko

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences; National Research University Higher School of Economics

Email: a.baranchikov@yandex.ru
119991, Moscow, Russia; 101000, Moscow, Russia

A. Yapryntsev

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: a.baranchikov@yandex.ru
119991, Moscow, Russia

A. Rodina

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: a.baranchikov@yandex.ru
119991, Moscow, Russia

A. Baranchikov

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: a.baranchikov@yandex.ru
119991, Moscow, Russia

V. Ivanov

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences; Moscow State University

Хат алмасуға жауапты Автор.
Email: a.baranchikov@yandex.ru
119991, Moscow, Russia; 119991, Moscow, Russia

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© Е.Д. Шейченко, А.Д. Япрынцев, А.А. Родина, А.Е. Баранчиков, В.К. Иванов, 2023