Synthesis, structure and optical properties of semiconductor perovskite nanoparticles CsBX3 (B = Pb, Mn; X = Br, Cl)

Мұқаба

Дәйексөз келтіру

Толық мәтін

Ашық рұқсат Ашық рұқсат
Рұқсат жабық Рұқсат берілді
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Аннотация

Currently, ABX3 nanoparticles (NPs) based on lead halides attract the attention due to their unique optical properties and a wide range of applications. The preparation of NPs with lead as a partial or complete replacement is particularly interesting because of the toxicity of this chemical element and most of its compounds. In this study, we propose a modified method for perovskite NPs synthesis using manganese as a partial replacement for lead. The results obtained describe the structures, shapes and dimensions of the synthesized nanoparticles. It has been shown that partial replacement of lead with manganese leads to the appearance of new photoluminescence bands in the region of 600 nm.

Толық мәтін

Рұқсат жабық

Авторлар туралы

V. Gushchina

Moscow Institute of Physics and Technology (National Research University); Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: ya.l2er0us0ya2012@ya.ru
Ресей, Dolgoprudny, 141701; Moscow, 119991

A. Son

Moscow Institute of Physics and Technology (National Research University); Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Хат алмасуға жауапты Автор.
Email: sonsacha@gmail.com
Ресей, Dolgoprudny, 141701; Moscow, 119991

A. Egorova

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
Ресей, Moscow, 119991

A. Arkhipenko

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
Ресей, Moscow, 119991

M. Teplonogova

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
Ресей, Moscow, 119991

N. Efimov

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
Ресей, Moscow, 119991

S. Kozyukhin

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
Ресей, Moscow, 119991

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2. Рис.1. ② : 1 – cspbbr3; 2 – cspbcl3–zbrz; 3 – cspbcl3; 4 – cspb1–ymnycl3–Zbrz; 5 – Cspb1–ymnycl3.

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3. Рис. 2. Микрофотографии наночастиц различных составов: CsPbBr3 (а); CsPbCl3–zbr you (б); CsPbCl3 (в); CsPb1–yMnyCl3–zbr you (г); CsPb1–yMnyCl3 (д).

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4. Fig. 3. ② : 1 – cspbbr3; 2 – cspbcl3–zbrz; 3 – cspbcl3; 4 – cspb1–ymnycl3–zbrz; 5 – Cspb1–Ymnycl3.

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5. Fig. 4. 6-cspbbr3; 2 – cspbcl3 – zbrz; 3–cspbcl3; 4 – cspb1 – ymnycl3–zbrz; 5–cspb1 – ymnycl3.

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6. Fig. 5. Photoluminescence spectra of nanoparticles: 1 – CsPbBr3 (λvozb = 365 nm); 2 – CsPbCl3–zBrz (λvozb = = 365 nm); 3 – CsPbCl3 (λvozb = 365 nm); 4 – CsPb1–yMnyCl3–zBrz (λvozb = 227 nm); 5 – CsPb1–yMnyCl3 (λvb = 241 nm).

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7. Fig. 6. EPR spectra for CsPb1–yMnyCl3 nanoparticles (X-band, 294 K).

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