Composite Aerogels Based on Reduced Graphene Oxide Decorated with Iron Oxide Nanoparticles: Synthesis, Physicochemical and Sorption Properties

E. A. Neskoromnaya; Нескоромная Е. А.; A. V. Babkin; Бабкин А. В.; E. A. Zakharchenko; Захарченко Е. А.; Yu. G. Morozov; Морозов Ю. Г.; E. N. Kabachkov; Кабачков Е. Н.; Yu. M. Shulga; Шульга Ю. М.

doi:10.31857/S0207401X23070130

Composite Aerogels Based on Reduced Graphene Oxide Decorated with Iron Oxide Nanoparticles: Synthesis, Physicochemical and Sorption Properties

Авторлар: Neskoromnaya E.A.¹, Babkin A.V.², Zakharchenko E.A.¹, Morozov Y.G.³, Kabachkov E.N.⁴, Shulga Y.M.⁴
Мекемелер:
1. Vernadsky Institute of Geochemistry and Analytical Chemistry, Russian Academy of Sciences
2. Department of Chemistry, Moscow State University
3. Merzhanov Institute of Structural Macrokinetics and Materials Science, Russian Academy of Sciences
4. Federal Research Center of Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences
Шығарылым: Том 42, № 7 (2023)
Беттер: 41-49
Бөлім: XXXIV СИМПОЗИУМ “СОВРЕМЕННАЯ ХИМИЧЕСКАЯ ФИЗИКА” (СЕНТЯБРЬ 2022 г., ТУАПСЕ)
URL: https://rjpbr.com/0207-401X/article/view/674851
DOI: https://doi.org/10.31857/S0207401X23070130
EDN: https://elibrary.ru/YFHLEQ
ID: 674851

Дәйексөз келтіру

Толық мәтін

Ашық рұқсат
Рұқсат жабық

Рұқсат берілді
Рұқсат жабық

Рұқсат ақылы немесе тек жазылушылар үшін

Аннотация
Авторлар туралы
Әдебиет тізімі
Қосымша файлдар
Статистика

Аннотация

In this study, aerogels based on graphene oxide decorated with iron oxide nanoparticles are obtained by drying in supercritical isopropanol. For the synthesized samples with the calculated initial iron contents of 9, 18 and 36 wt %, the morphology and structure of the graphene matrix and iron-containing nanoparticles are studied using the scanning electron microscopy (SEM) and transmission electron microscopy (TEM) methods. Comparative investigations are conducted to analyze the carbon and hydrogen composition within the synthesized aerogels structure, followed by an assessment of their magnetic properties at ambient temperature. Sorption experiments are carried out for the extraction of heavy and rare earth elements from multicomponent aqueous solutions of a complex composition.

Негізгі сөздер

graphene oxide, iron oxide nanoparticles, supercritical drying, aerogel, magnetization, sorption properties

Әдебиет тізімі

Häder D.-P., Banaszak A.T., Villafañe V.E. et al. // Sci. Total Environ. 2020. V. 713. P. 136586; https://doi.org/10.1016/j.scitotenv.2020.136586
Thompson L.A., Darwish W.S. // J. Toxicol. 2019. V. 2019. P. 2345283; https://doi.org/10.1155/2019/2345283
Boretti A., Rosa L. // npj Clean Water. 2019. V. 2. P. 15; https://doi.org/10.1038/s41545-019-0039-9
Конькова Т.В., Гордиенко М.Г., Меньшутина Н.В. и др. // Сверхкритические флюиды: теория и практика. 2017. Т. 12. № 3. С. 32.
Ali I., Neskoromnaya E.A., Melezhik A.V. et al. J. Porous. Mater. 2022. V. 29. P. 545; https://doi.org/10.1007/s10934-021-01175-0
Liu H., Qiu H. // Chem. Eng. J. 2020. V. 393. P. 124 691; https://doi.org/10.1016/j.cej.2020.124691
Вальчук Н.А., Бровко О.С., Паламарчук И.А. и др. // Сверхкритические флюиды: теория и практика. 2018. Т. 13. № 3. С. 83; https://doi.org/10.34984/SCFTP.2018.13.3.009
Zhang X., Zhou J., Zheng Y., Wei H., Su Z. // Chem. Eng. J. 2021. V. 420. Part 1. P. 129700; https://doi.org/10.1016/j.cej.2021.129700
Neskoromnaya E.A., Burakov A.E., Melezhik A.V. et al. // Inorg. Mater. Appl. Res. 2020. V. 11. № 2. P. 467; https://doi.org/10.1134/S2075113320020264
Guo H., Jiao T., Zhang Q. et al. // Nanoscale Res. Lett. 2015. V. 10. P. 272; https://doi.org/10.1186/s11671-015-0931-2
Huong P., Tu N., Lan H. et al. // RSC Adv. 2018. Issue 22. P. 12 376; https://doi.org/10.1039/C8RA00270C
Wang S., Ning H., Hu N. et al. // Composites, Part B. 2019. V. 163. P. 716; https://doi.org/10.1016/j.compositesb.2018.12.140
Abd-Elhamid A.I., Kamoun E.A., El-Shanshory A.A. // Mol. Liq. 2019. V. 279. P. 530; https://doi.org/10.1016/j.molliq.2019.01.162
Губин С.П., Буслаева Е.Ю. // Сверхкритические флюиды: теория и практика. 2009. Т. 4. № 4. С. 73.
Neskoromnaya E.A., Khamizov R.K., Melezhyk A.V. et al. // Colloids Surf., A. 2022. V. 655. P. 130224; https://doi.org/10.1016/j.colsurfa.2022.130224
Shul’ga Yu.M., Kabachkov E.N. et al. // Russ. J. Phys. Chem. A. 2019. V. 93(2). P. 296; https://doi.org/10.1134/S0036024419010278
Thakur A., Kumar S., Rangra V.S. // Proc. AIP Conf. 2015. V. 1661. P. 080032; https://doi.org/10.1063/1.4915423
Khandare L., Late D.J. // Appl. Surf. Sci. 2017. V. 418. Part A. P. 2; https://doi.org/10.1016/j.apsusc.2016.11.199
Khamboonrueang D. et al. // Mater. Res. Bull. 2018. V. 107. P. 236.
Paganin V.A., Ticianelli E.A., Gonzalez E.R. // J. Appl. Elecrochem. 1996. V. 26. P. 297.
Lv P., Tang X., Zheng R. et al. // Nanoscale Res. Lett. 2017. V. 12. P. 630; https://doi.org/10.1186/s11671-017-2395-z
Aliahmad M., Nasiri Moghaddam N. // Mater. Sci-Pol. 2013. V. 31. № 264; https://doi.org/10.2478/s13536-012-0100-6
Shulga Y.M., Melezhik A.V., Kabachkov E.N. et al. // Appl. Phys. A: Mater. Sci. Process. 2019. V. 125. P. 460.
Ravi T., Sundararaman S. // Russ. J. Phys. Chem. B. 2021. V. 15. P. 462; https://doi.org/10.1134/S1990793121030295
Lei Y., Chen F., Luo Y. et al. // J. Mater. Sci. 2014. V. 49. P. 4236; https://doi.org/10.1007/s10853-014-8118-2
Chen W., Li S., Chen C., Yan L. // Adv. Mater. 2011. V. 23. Issue 47. P. 5679; https://doi.org/10.1002/adma.201102838
Wang T., Zhang L., Wang H. et al. // ACS Appl. Mater. Interfaces. 2013. V. 5. № 23. P. 12449; https://doi.org/10.1021/am403533v
Kumar S., Nair R.R., Pillai P.B. et al. Ibid. 2014. V. 6. № 20. P. 17426; https://doi.org/10.1021/am504826q